{"id":148,"date":"2018-07-25T14:28:26","date_gmt":"2018-07-25T13:28:26","guid":{"rendered":"https:\/\/research.reading.ac.uk\/spectroelectrochemistry\/?page_id=148"},"modified":"2019-04-26T14:02:53","modified_gmt":"2019-04-26T13:02:53","slug":"low-temperature-ottle-cell","status":"publish","type":"page","link":"https:\/\/research.reading.ac.uk\/spectroelectrochemistry\/optically-transparent-thin-layer-electrochemical-cells\/low-temperature-ottle-cell\/","title":{"rendered":"Low Temperature OTTLE cell"},"content":{"rendered":"<p>Low temperature Spectroelectrochemistry not only helps study unstable electro-generated intermediates at room temperature, but also serves to investigate temperature-dependent properties of complexes. The first successful prototype of the unique Low Temperature OTTLE cell covering the whole UV-Vis-NIR-IR region was described in <em>Applied Spectroscopy<\/em> <strong>1994<\/strong>, 48, 1522. Version 1 has since been cited in 81 publications while Version 2 (with CaF<sub>2<\/sub> windows) has been cited in 41 publications. A significantly improved smaller commercial version of the low temperature OTTLE cell is now available (<em>Collect. Czech. Chem. Commun.<\/em> <strong>2003<\/strong>, 68, 1687). To date this cell has been employed in seven different laboratories in the UK, Germany, Italy, India and Australia.<\/p>\n<h2>Low Temperature OTTLE cell features<\/h2>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"alignright wp-image-175 size-medium\" style=\"letter-spacing: 0.08px\" src=\"https:\/\/research.reading.ac.uk\/spectroelectrochemistry\/wp-content\/uploads\/sites\/66\/images\/Low-Temperature-Optically-Transparent-Thin-Layer-Electrochemical-Cell-176x300.png\" alt=\"Various Low Temperature OTTLE Cell setups\" width=\"176\" height=\"300\" srcset=\"https:\/\/research.reading.ac.uk\/spectroelectrochemistry\/wp-content\/uploads\/sites\/66\/images\/Low-Temperature-Optically-Transparent-Thin-Layer-Electrochemical-Cell-176x300.png 176w, https:\/\/research.reading.ac.uk\/spectroelectrochemistry\/wp-content\/uploads\/sites\/66\/images\/Low-Temperature-Optically-Transparent-Thin-Layer-Electrochemical-Cell.png 366w\" sizes=\"auto, (max-width: 176px) 100vw, 176px\" \/><\/p>\n<p>In addition to many of the features of our <a href=\"https:\/\/research.reading.ac.uk\/spectroelectrochemistry\/optically-transparent-thin-layer-electrochemical-cells\/room-temperature-ottle-cell\/\">Room Temperature OTTLE cell<\/a>, our Low Temperature OTTLE cell offers some unique advantages for temperature dependent measurements.<\/p>\n<p><span class=\"emphasise\"><strong><span style=\"color: #000000\">Advanced, Iterative Design:<\/span><\/strong><\/span><\/p>\n<p>The product of more than 20 years of iterative design, we are proud to now be able to offer our user&#8217;s a cryostatted version of our extremely successful room temperature cell.\u00a0 In combination with the commercially available cryostat Optistat DN (<a href=\"https:\/\/nanoscience.oxinst.com\/products\/cryostats-for-spectroscopy\/optistatdn\">OxfordInstruments<\/a>), our cell boasts:<\/p>\n<ul>\n<li>An effective operating range of between 298 and 175 K.<\/li>\n<li>Efficient and accurate temperature control (elevation and cooling) to within 1 K by using local electronic temperature control.<\/li>\n<li>Crossed pairs of CaF<sub>2<\/sub> (for IR) and Quartz (for UV-VIS) windows. <span style=\"color: #800000\"><strong>Coming in 2019, Version 3 &#8211; with diverse window materials!\u00a0<\/strong><\/span><\/li>\n<li>Rapid &amp; complete electrolysis; even close to low temperature limits of electrolytes.<\/li>\n<\/ul>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-medium wp-image-288\" src=\"https:\/\/research.reading.ac.uk\/spectroelectrochemistry\/wp-content\/uploads\/sites\/66\/Unorganized\/low-temperature-cell-300x212.png\" alt=\"\" width=\"300\" height=\"212\" srcset=\"https:\/\/research.reading.ac.uk\/spectroelectrochemistry\/wp-content\/uploads\/sites\/66\/Unorganized\/low-temperature-cell-300x212.png 300w, https:\/\/research.reading.ac.uk\/spectroelectrochemistry\/wp-content\/uploads\/sites\/66\/Unorganized\/low-temperature-cell.png 503w\" sizes=\"auto, (max-width: 300px) 100vw, 300px\" \/><\/p>\n<h4><\/h4>\n<h2>Obtain a quote<\/h2>\n<p><a href=\"https:\/\/research.reading.ac.uk\/spectroelectrochemistry\/faq\/\">Contact us to discuss your requirements and obtain a quote for one of our Low Temperature OTTLE cells<\/a><\/p>\n","protected":false},"excerpt":{"rendered":"<p>Cited in more than 50 publications, a significantly improved, smaller commercial version of our Low Temperature OTTLE cell is now available.<\/p>\n","protected":false},"author":8,"featured_media":200,"parent":141,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"_acf_changed":false,"_monsterinsights_skip_tracking":false,"_monsterinsights_sitenote_active":false,"_monsterinsights_sitenote_note":"","_monsterinsights_sitenote_category":0,"__cvm_playback_settings":[],"__cvm_video_id":"","footnotes":""},"class_list":["post-148","page","type-page","status-publish","has-post-thumbnail","hentry"],"acf":[],"yoast_head":"<!-- This site is optimized with the Yoast 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